Pii: S0040-6090(99)00023-1

نویسندگان

  • Qiang Fu
  • Chuan-Bao Cao
  • He-Sun Zhu
چکیده

A new sol±gel route was applied to prepare alumina ®lms by using AlCl3 ́6H2O as starting material and acetylacetone (AcAc) as additive. Our research results show that AcAc and aluminum form a complex compound in the sol, which makes the sol very stable. Meanwhile, the complex structure prevents the decomposition going on quickly during the sintering process and the obtained ®lms are free of cracks. The asprepared ®lms were amorphous. When the sintering temperature reached up to 6008C, g-Al2O3 began to form and was transformed to a Al2O3 at temperatures over 1200 8C. q 1999 Elsevier Science S.A. All rights reserved.

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تاریخ انتشار 1999